Institut für Experimentelle und Angewandte Physik der
Christian-Albrechts-Universität zu Kiel

Department Solid State Physics

Physics of Biological Composite Materials

Institut für Experimentelle und Angewandte Physik Universität Kiel

 

 

Publications

 
Publications
 
.

PhD theses

Influence of water on the mechanical properties of wood investigated using X-ray and neutron scattering, Ingo Grotkopp, 2006
Morphologie und mechanische Eigenschaften von Zellulosefasern: Untersuchungen mit Röntgen- und Neutronenstreuung, Klaas Kölln, 2004
 

Peer-reviewed articles in journals, books and conference proceedings

submitted

[80] T. Seydel, D. Sapede, M. M. Koza, M. Müller, F. Vollrath, C. Riekel.
Molecular mobility of spider dragline silk and adsorbed water studied by neutron spectroscopy techniques.
Macromolecules, submitted.

2008 and in press

[79] M. Müller.
Synchrotron radiation X-ray scattering techniques for studying the micro- and nanostructure of wood and their relation to the mechanical properties.
In: P. Kettunen, editor, Advances in materials science of wood, Trans Tech Publications Ltd., Switzerland, in press.
[78] D. Cazorla-Amorós, D. Lozano-Castelló, M. Müller.
Application of non-crystalline diffraction with microfocus to carbon fibres.
In: M. C. Garcia-Gutiérrez, A. Nogales, M. A. Goméz, T. A. Ezquerra, editors, Applications of synchrotron light to non-crystalline diffraction in materials and life sciences, Lecture Notes in Physics, Springer, Berlin, in press.
[77] B. M. Murphy, M. Müller, J. Stettner, H. Requardt, J. Serrano, M. Krisch, W. Press.
Investigating surface dynamics with inelastic X-ray scattering.
J. Phys. Condens. Matt., in press.
[76] I. Krasnov, I. Diddens, N. Hauptmann, G. Helms, M. Ogurreck, T. Seydel, S.S. Funari, M. Müller.
Mechanical properties of silk: Interplay of deformation on macroscopic and molecular length scales.
Phys. Rev. Lett., 100:048104, 2008.
[75] M. Peura, M. Müller, U. Vainio, M.-P. Sarén, P. Saranpää, R. Serimaa.
X-ray microdiffraction reveals the orientation of cellulose microfibrils and the size of cellulose crystallites in single Norway spruce tracheids.
Trees, 22:49-61, 2008.

2007

[74] D. Loidl, O. Paris, H. Rennhofer, M. Müller, H. Peterlik.
Skin-core structure and bimodal Weibull distribution of the strength of carbon fibers.
Carbon, 45:2801-2805, 2007.
[73] M. Müller, B. Murphy, M. Burghammer, C. Riekel, E. Pantos, J. Gunneweg.
Ageing of native cellulose fibres under archaeological conditions: Textiles from the Dead Sea region studied using X-ray microdiffraction.
Appl. Phys. A, 89:877-881, 2007.
[72] M. Peura, K. Kölln, I. Grotkopp, P. Saranpää, M. Müller, R. Serimaa.
The effect of tension on the structure of normally grown Norway spruce.
Wood Sci. Technol., 41:565-583, 2007.
[71] T. Seydel, K. Kölln, I. Krasnov, I. Diddens, N. Hauptmann, G. Helms, M. Ogurreck, S.-G. Kang, M.M. Koza, M. Müller.
Silkworm silk under strain investigated by X-ray diffraction and neutron spectroscopy.
Macromolecules, 40:1035-1042, 2007.

2006

[70] J. Gunneweg, M. Balla, J. Wouters, C. Greenblatt, M. Müller, E. Pantos, H. van der Plicht, A. Adriaens, K.L. Rasmussen, C. Riekel, M. Burghammer, and B. Murphy.
A multi-interdisciplinary handshake between humanities and science at Qumran.
In: A. Denker, A. Adriaens, M. Dowsett, A. Guimlia-Mair, Eds., COST Action G8: Non-destructive testing and analysis of museum objects, pp.185-193, Fraunhofer IRB Verlag, 2006.
[69] M. Müller, M. Burghammer, J. Sugiyama.
Direct investigation of the structural properties of tension wood cellulose microfibrils using microbeam X-ray fibre diffraction.
Holzforschung, 60:474-479, 2006.
[68] M. Müller, B. Murphy, M. Burghammer, C. Riekel, J. Gunneweg, E. Pantos.
Structural and elemental analysis of single textile fibres from Qumran using modern synchrotron radiation X-ray microdiffraction and microfluorescence techniques.
In: J. Gunneweg, C. Greenblatt, A. Adriaens, Eds., Bio- and materials culture at Qumran, COST Action G8, pp. 109-123, Fraunhofer IRB Verlag, 2006.
[67] M. Müller, B. Murphy, M. Burghammer, I. Snigireva, C. Riekel, J. Gunneweg, E. Pantos.
Identification of single archaeological textile fibres from the Cave of Letters using synchrotron radiation microbeam diffraction and microfluorescence.
Appl. Phys. A, 83:183-188, 2006.
[66] M. Peura, I. Grotkopp, H. Lemke, A. Vikkula, J. Laine, M. Müller, R. Serimaa.
Negative Poisson ratio of crystalline cellulose in sulphate cooked Norway spruce.
Biomacromolecules, 7:1521-1528, 2006.
[65] D. Lozano-Castelló, D. Cazorla-Amorós, J.-A. Maciá-Agulló, A. Linares-Solano, M. Müller, M. Burghammer, C. Riekel.
Isotropic and anisotropic microporosity development upon chemical actication of carbon fibres, revealed by microbeam small-angle scattering.
Carbon
, 44:1121-1129, 2006.

2005

[64] B. M. Murphy, H. Requardt, J. Stettner, J. Serrano, M. Krisch, M. Müller, W. Press.
Phonon modes at the 2H-NbSe2 surface observed by surface sensitive inelastic X-ray scattering.
Phys. Rev. Lett., 95:256104, 2005.
[63] M. Peura, M. Müller, R. Serimaa, U. Vainio, M.-P.Sarén, P. Saranpää, M. Burghammer.
Structural studies of single wood cell walls by synchrotron X-ray microdiffraction and polarised light.
Nucl. Instrum. Meth. B, 238:16-20, 2005.
[62] D. Loidl, H. Peterlik, O. Paris, M. Müller, M. Burghammer, C. Riekel.
Structure and mechanical properties of carbon fibres: A review of recent microbeam diffraction studies with synchrotron radiation.
J. Synchr. Rad., 12:758-764, 2005.
[61] K. Kölln, I. Grotkopp, M. Burghammer, S. V. Roth, S. S. Funari, M. Dommach, M. Müller.
Mechanical properties of cellulose fibres and wood - Orientational aspects in situ investigated with synchrotron radiation.
J. Synchr. Rad., 12:739-744, 2005.
[60] J. Baumert, C. Gutt, M. Krisch, H. Requardt, M. Müller, J. S. Tse, D. D. Klug, W. Press.
Elastic properties of methane hydrate at high pressures.
Phys. Rev. B, 72:054302, 2005.
[59] J. Keckes, I. Burgert, M. Müller, K. Kölln, M. Hamilton, M. Burghammer, S. V. Roth, S. E. Stanzl-Tschegg, P. Fratzl.
In situ WAXS studies on structural changes in wood foils and in individual wood cells during microtensile tests.
Fibre Diffraction Review, 13:48-51, 2005.

2004

[58] M. Peura, R. Serimaa, M. Müller, M.-P. Sarén, P. Saranpää.
The orientation of cellulose microfibrils in single tracheids and solid wood samples as investigated by x-ray diffraction.
In U. Schmitt, P. Ander, J. R. Barnett, A. M. C. Emons, G. Jeronimides, P. Saranpää, editors, Wood fibre cell walls: Methods to study their function, structure and properties, pages 141-150, SLU, Uppsala, 2004.
[57] M. Müller, B. Murphy, M. Burghammer, C. Riekel, M. Roberts, M. Papiz, D. Clarke, J. Gunneweg, E. Pantos.
Indentification of ancient textile fibres from Khirbet Qumran caves using synchrotron radiation microbeam diffraction.
Spectrochim. Acta B, 59(10-11):1669-1674, 2004.
[56] T. Koponen, M. Peura, T. Karppinen, E. Haeggström, M. Müller, P. Saranpää, R. Serimaa.
Elastic properties and cell wall structure of Norway spruce as a function of year ring.
In: S. E. Stanzl-Tschegg, M. Gindl, G. Sinn, editors, Proceedings of the 2nd International Symposium on Wood Machining, pages ??-??, Wien, 2004.
[55] J. Keckes, I. Burgert, K. Frühmann, M. Müller, K. Kölln, M. Hamilton, M. Burghammer, S. V. Roth, S. Stanzl-Tschegg, P. Fratzl.
In-situ synchrotron studies of sructural changes in wood during microtensile tests.
In: S. E. Stanzl-Tschegg, M. Gindl, G. Sinn, editors, Proceedings of the 2nd International Symposium on Wood Machining, pages 37-44, Wien, 2004.
[54] D. Loidl, O. Paris, M. Müller, M. Burghammer, C. Riekel, K. Kromp and H. Peterlik.
Nanostructure of single carbon fibers investigated with synchrotron radiation In: P. J. M. Bartos, J. J. Highes, P. Trtik, W. Zhu, editors, Nanotechnology in Construction, pages 205-214. The Royal Society of Chemistry, Cambridge, 2004.

2003

[53] M. Burghammer, M. Müller, and C. Riekel.
X-ray synchrotron radiation microdiffraction on fibrous biopolymers like cellulose and in particular spider silk.
Recent Res. Devel. Macromol.
, 7:103-125, 2003.
[52] J. Keckes, I. Burgert, K. Frühmann, M. Müller, K. Kölln, M. Hamilton, M. Burghammer, S. V. Roth, S. Stanzl-Tschegg and P. Fratzl.
Cell-wall recovery after irreversible deformation of wood.
Nature Mater., 2:810-814, 2003
[51] J. Baumert, C. Gutt, V. P. Shpakov, J. S. Tse, M. Krisch, M. Müller, H. Requardt, D. D. Klug, S. Janssen, and W. Press.
Lattice dynamics of methane hydrate: observation of symmetry avoided crossing by experiment and theory.
Phys. Rev. B
, 68:174301, 2003.
[50] B. Murphy, J. Stettner, M. Traving, M. Sprung, I. Grotkopp, M. Müller, M. Tolan, C. S. Oglesby, and W. Press.
Surface behaviour at the charge density wave transition in NbSe2.
Physica B
, 336:103-108, 2003.
[49] J.-F. Blachot, O. Diat, J.-L. Putaux, A.-L. Rollet, L. Rubatat, C. Vallois, M. Müller, and G. Gebel.
Anisotropy of structure and transport properties in sulfonated polyimide membranes.
J. Memb. Sci. 214:31-42, 2003.
[48] H. Lichtenegger, M. Müller, R. Wimmer, and P. Fratzl.
Microfibril angles inside and outside crossfields of norway spruce tracheids.
Holzforschung
, 57:13-20, 2003.
[47] M. Müller, M. Z. Papiz, D. T. Clarke, M. A. Roberts, B. M. Murphy, M. Burghammer, C. Riekel, E. Pantos, and J. Gunneweg.
Identification of the textiles using microscopy and synchrotron radiation x-ray fibre diffraction.
In: Jean-Baptiste Humbert and Jan Gunneweg, editors, Khirbet Qumrân et 'Aïn Feshkha, Vol. II - Studies of Anthropology, Physics and Chemistry, Chapter XII, pages 277-286. Academic Press, Fribourg, Vandenhoeck & Ruprecht, Göttingen, 2003.
[46] O. Paris and M. Müller.
Scanning x-ray microdiffraction of complex materials: Diffraction geometry considerations.
Nucl. Instrum. Meth. B
, 200:390-396, 2003.
[45] D. Loidl, H. Peterlik, M. Müller, C. Riekel, and O. Paris.
Elastic moduli of nanocrystallites in carbon fibers measured by in situ x-ray microbeam diffraction.
Carbon
, 41:563-570, 2003.

2002

[44] J. Laï Kee Him, H. Chanzy, M. Müller, J.-L. Putaux, T. Imai, and V. Bulone.
In vitro
versus in vivo cellulose microfibrils from plant primary wall synthases: structural differences.
J. Biol. Chem.
, 277:36931-36939, 2002.
[43] R. Hori, M. Müller, U. Watanabe, H. C. Lichtenegger, P. Fratzl, and J. Sugiyama.
The importance of seasonal differences in the cellulose microfibril angle in softwoods in determining acoustic properties.
J. Mater. Sci.
, 37:4279-4284, 2002.
[42] C. E. Moss, M. F. Butler, M. Müller, and R. E. Cameron.
Microfocus small-angle x-ray scattering investigation of the skin-core microstructure of lyocell cellulose fibers.
J. Appl. Polym. Sci.
, 83:2799-2816, 2002.
[41] M. Müller, R. Hori, T. Itoh, and J. Sugiyama.
X-ray microbeam and electron diffraction experiments on developing xylem cell walls.
Biomacromolecules
, 3:182-186, 2002.
[40] Y. Nishiyama, H. Chanzy, M. Wada, J. Sugiyama, K. Mazeau, T. Forsyth, C. Riekel, M. Müller, B. Rasmussen, and P. Langan.
Synchrotron x-ray and neutron fiber diffraction studies of cellulose polymorphs.
Adv. X-ray Anal.
, 45:385-390, 2002.
[39] O. Diat, J.-F. Blachot, A.-L. Rollet, L. Rubatat, C. Vallois, M. Müller, and G. Gebel.
Anisotropie structurale et des propriétés de transport dans les membranes en polyimide sulfoné.
J. Phys. IV - Proc.
, 12:Pr2-63-Pr2-71, 2002.
[38] D. Lozano-Castelló, E. Raymundo-Piñero, D. Cazorla-Amorós, A. Linares-Solano, M. Müller, and C. Riekel.
Characterization of pore distribution in activated carbon fibers by microbeam small-angle x-ray scattering.
Carbon
, 40:2727-2735, 2002.
[37] D. Lozano-Castelló, E. Raymundo-Piñero, D. Cazorla-Amorós, A. Linares-Solano, M. Müller, and C. Riekel.
Microbeam small-angle x-ray scattering (µSAXS): A novel technique for the characterization of activated carbon fibers.
In F. Rodríguez-Reinero, B. McEnaney, J. Rouquerol, and K. Unger, editors, Characterisation of Porous Solids VI, volume 144 of Studies in Surface Science and Catalysis, pages 51-58. Elsevier Science, 2002.

2001

[36] M. Müller, M. Burghammer, and C. Riekel.
Combined scanning microdiffraction and micro small-angle scattering at the microfocus beamline ID13 at the ESRF.
Nucl. Instrum. Meth. A
, 467-468:958-961, 2001.
[35] O. Paris, D. Loidl, M. Müller, H. Lichtenegger, and H. Peterlik.
Cross-sectional texture of carbon fibers analysed by scanning microbeam x-ray diffraction.
J. Appl. Cryst.
, 34:473-479, 2001.
[34] C. Riekel, C. L. Craig, M. Burghammer, and M. Müller.
Microstructural homogeneity of dragline silk spun by Eriophora fuligenea (C. L. Koch).
Naturwissenschaften
, 88:67-72, 2001.

2000

[33] C. Czihak, M. Müller, H. Schober, and G. Vogl.
Ice formation in amorphous cellulose.
Physica B
, 276-278:286-287, 2000.
[32] C. Czihak, M. Müller, H. Schober, and G. Vogl.
Relaxational motion and ice formation of water adsorbed to cellulose.
J. Phys. IV - Proc.
, 10:Pr7-199-Pr7-202, 2000.
[31] R. Hori, J. Sugiyama, T. Itoh, and M. Müller.
Synchrotron x-ray diffraction analysis of cellulose in developing xylem cell walls from cryptomeria japonica.
Wood Research
, 87:19-20, 2000.
[30] H. Lichtenegger, A. Reiterer, S. E. Tschegg, M. Müller, C. Riekel, O. Paris, and P. Fratzl.
Microfibril angle and mechanical properties of wood.
In: H. Ch. Spatz and Th. Speck, editors, Proceedings of the 3rd Plant Biomechanics Conference, pages 436-442, Stuttgart, New York, 2000. Georg Thieme.
[29] H. Lichtenegger, A. Reiterer, S. E. Tschegg, M. Müller, O. Paris, and P. Fratzl.
Cellulose orientation in the wood cell wall.
In: J.E. Stanzl-Tschegg, A. Reiterer, editors, Proceedings of the International Symposium on Wood Machining, pages 31-37, Wien, 2000.
[28] M. Müller, C. Riekel, R. Vuong, and H. Chanzy.
Skin/core micro-structure in viscose rayon fibers analysed by x-ray microbeam and electron diffraction mapping.
Polymer
, 41:2627-2632, 2000.
[27] M. Müller, C. Czihak, H. Schober, Y. Nishiyama, and G. Vogl.
All disordered regions of native cellulose show common low-frequency dynamics.
Macromolecules
, 33:1834-1840, 2000.
[26] M. Müller, C. Czihak, M. Burghammer, and C. Riekel.
Combined x-ray microbeam small-angle scattering and fibre diffraction experiments on single native cellulose fibres.
J. Appl. Cryst.
, 33:817-819, 2000.
[25] S. Di Fonzo, W. Jark, S. Lagomarsino, C. Giannini, L. De Caro, A. Cedola, and M. Müller.
Non-destructive determination of local strain with 100 nanometer spatial resolution.
Nature
, 403:638-640, 2000.
[24] J. C. Garson, F. Baltenneck, F. Leroy, C. Riekel, and M. Müller.
Histological structure of human nail as studied by synchrotron x-ray microdiffraction.
Cell. Mol. Biol.
, 46:1025-1034, 2000.
[23] M. Müller, M. Burghammer, D. Flot, C. Riekel, C. Morawe, B. Murphy, and A. Cedola.
Microcrystallography with an x-ray waveguide.
J. Appl. Cryst.
, 33:1231-1240, 2000.
[22] O. Paris, D. Loidl, H. Peterlik, M. Müller, H. Lichtenegger, and P. Fratzl.
The internal structure of single carbon fibers determined by simultaneous small- and wide-angle x-ray scattering.
J. Appl. Cryst.
, 33:695-699, 2000.
[21] C. Riekel, M. Burghammer, and M. Müller.
Microbeam small-angle scattering experiments and their combination with microdiffraction.
J. Appl. Cryst.
, 33:421-423, 2000.

1999

[20] C. Czihak, M. Müller, H. Schober, L. Heux, and G. Vogl.
Dynamics of water adsorbed to cellulose.
Physica B
, 266:87-91, 1999.
[19] H. Lichtenegger, M. Müller, O. Paris, C. Riekel, and P. Fratzl.
Imaging of the helical arrangement of cellulose fibrils in wood by synchrotron x-ray microdiffraction.
J. Appl. Cryst.
, 32:1127-1133, 1999.
[18] M. Müller, M. Burghammer, and C. Riekel.
Fiber diffraction and small-angle scattering on single cellulose fibers.
ESRF Newsletter, 33:12-13, 1999.
[17] Y. Nishiyama, A. Isogai, T. Okano, M. Müller, and H. Chanzy.
Intra-crystalline deuteration of native cellulose.
Macromolecules
, 32:2078-2081, 1999.
[16] C. Riekel, C. Bränden, C. Craig, C. Ferrero, F. Heidelbach, and M. Müller.
Aspects of x-ray diffraction on single spider fibers.
Int. J. Biol. Macromol.
, 24:179-186, 1999.
[15] C. Riekel, M. Müller, and F. Vollrath.
In situ x-ray diffraction during forced silking of spider silk.
Macromolecules
, 32:4464-4466, 1999.
[14] J. Senker, H. Jacobs, M. Müller, W. Press, and G. Neue.
Reorientational dynamics of amide ions in isotypic phases of strontium and calcium amide. 2. Solid state NMR.
J. Phys. Chem. B
, 103:4497-4507, 1999.
[13] J. Senker, H. Jacobs, M. Müller, W. Press, H. M. Mayer, and R. M. Ibberson.
Structure determination of a low temperature phase of calcium and strontium amide by means of neutron powder diffraction on Ca(ND2)2 and Sr(ND2)2.
Z. Anorg. Allg. Chemie
, 625:2025-2032, 1999.

1998

[12] M. Müller, C. Czihak, G. Vogl, P. Fratzl, H. Schober, and C. Riekel.
Direct observation of microfibril arrangement in a single native cellulose fiber by microbeam small-angle x-ray scattering.
Macromolecules
, 31:3953-3957, 1998.
[11] M. Müller, B. Asmussen, W. Press, J. Senker, H. Jacobs, H. Büttner, and H. Schober.
Orientational order and rotational dynamics of the amide ion in potassium amide. II: Quasielastic and inelastic neutron scattering.
J. Chem. Phys.
, 109:3559-3567, 1998.
[10] J. Senker, H. Jacobs, M. Müller, W. Press, P. Müller, H. M. Mayer, and R. M. Ibberson.
Reorientational dynamics of amide ions in isotypic phases of strontium and calcium amide. 1. Neutron diffraction experiments.
J. Phys. Chem. B
, 102:931-940, 1998.

1997

[9] M. Müller, G. Vogl, H. Schober, H. Chanzy, and L. Heux.
Inelastic neutron scattering study on different types of cellulose.
In S. Cusack, H. Büttner, M. Ferrand, P. Langan, and P. Timmins, editors, Biological Macromolecular Dynamics, pages 99-103. Adenine Press, 1997.
[8] M. Müller, B. Asmussen, W. Press, J. Senker, H. Jacobs, H. Büttner, W. Kockelmann, and R. M. Ibberson.
Dynamics of the amide ions in potassium amide: Orientational order and disorder.
Physica B
, 234-236:45-47, 1997.
[7] M. Müller, J. Senker, W. Press, B. Asmussen, H. Jacobs, W. Kockelmann, H. M. Mayer, and R. M. Ibberson.
Orientational order and rotational dynamics of the amide ion in potassium amide. I: Neutron diffraction.
J. Chem. Phys.
, 107:2363-2373, 1997.
[6] J. Senker, M. Müller, W. Press, H. M. Mayer, R. M. Ibberson, and H. Jacobs.
Structure determination and reorientational disorder in two phases of Sr(ND2)2 and Ca(ND2)2.
Physica B
, 234-236:51-53, 1997.

1993-96

[5] B. Asmussen, M. Prager, M. Müller, D. Balszunat, W. Press, and C. J. Carlile.
Rotational excitations of symmetric top in cubic orientational potentials. II: CHD3 matrix-isolated in argon.
J. Chem. Phys.
, 105:1764-1769, 1996.
[4] B. Asmussen, M. Müller, D. Balszunat, W. Press, M. Prager, and C. J. Carlile.
Rotational excitations of the symmetric top molecule CHD3 in rare gas crystals.
Physica B
, 226:224-227, 1996.
[3] D. Balszunat, B. Asmussen, M. Müller, W. Press, W. Langel, G. Coddens, M. Ferrand, and H. Büttner.
Rotational excitations of methane molecules in porous media.
Physica B
, 226:185-188, 1996.
[2] W. Press, D. Bahr, M. Tolan, B. Burandt, M. Müller, P. Müller-Buschbaum, V. Nitz, and J. Stettner.
X-ray diffraction from mesoscopic systems.
Physica B
, 198:42-47, 1994.
[1] M. Müller, D. Bahr, W. Press, R. Jebasinski, and S. Mantl.
Annealing of silicon implanted by a high dose of cobalt ions investigated by in situ x-ray diffraction.
J. Appl. Phys.
, 74:1590-1596, 1993.